GLC-Mass Spectral Analysis of Psilocin and Psilocybin
David B. Repke, Dale Thomas Leslie, Daniel Mandell, Nicholas G. Kish
Journal of Pharmaceutical Sciences May 1, 1977 DOI: 10.1002/jps.2600660539 (opens in new tab)
Study at a glance
AI-extracted from the abstract| Characteristics | Method development and analytical study Peer reviewed |
|---|---|
| Population | Extract of Psilocybe cubensis (Earle) Sing. |
| Topics | Psilocybin |
| Keywords | Hallucinogen Mass spectrometry Spectral analysis Trimethylsilyl Chromatography Stereochemistry |
| Citations | 31 |
| Key points | The combined GLC-mass spectrometry technique with trimethylsilyl derivatization successfully analyzed psilocin and psilocybin in an extract of Psilocybe cubensis. |
Abstract
With the combined technique of GLC-mass spectrometry, psilocin and psilocybin, two hallucinogenic indoles, were analyzed as their trimethylsilyl derivatives. The method was applied to these two components in an extract of Psilocybe cubensis (Earle) Sing.
Citations in the library
Cited by 18
- Morphological and chemical analysis of magic mushrooms in Japan. Forensic Science International December 17, 2003
- Quantitative analysis of psilocybin and psilocin and psilocybe baecystis (singer and smith) by high-performance liquid chromatography and by thin-layer chromatography Journal of Chromatography A March 1, 1981
- Analysis of psilocybin and psilocin in Psilocybe subcubensis GUZMÁN by ion mobility spectrometry and gas chromatography–mass spectrometry Forensic Science International 1999
- The Determination of Psilocin and Psilocybin in Hallucinogenic Mushrooms by HPLC Utilizing a Dual Reagent Acidic Potassium Permanganate and Tris(2,2′‐bipyridyl)ruthenium(II) Chemiluminescence Detection System Journal of Forensic Sciences 2006
- Occurrence and use of hallucinogenic mushrooms containing psilocybin alkaloids TemaNord May 19, 2009
and 13 more in the library