Abstract A sensitive semi‐micro column high‐performance liquid chromatography with fluorescence detection method was developed for the determination of 3,4‐methylenedioxymethamphetamine (MDMA), 3,4‐methylenedioxyamphetamine (MDA), methamphetamine (MP) and amphetamine (AP) in human hair. 4‐(4,5‐Diphenyl‐1 H ‐imidazol‐2‐yl)benzoyl chloride (DIB‐Cl) and 1‐methyl‐3‐phenylpropylamine were used as...
Abstract A simultaneous semi‐micro column HPLC method with fluorescence detection of abused drugs, such as 3,4‐methylenedioxymethamphetamine (MDMA), 3,4‐methylenedioxyamphetamine (MDA), amphetamine (AP) and methamphetamine (MP) in rat urine was examined by using 4‐( N , N ‐dimethylaminosulphonyl)‐7‐fluoro‐1,2,3‐benzoxadiazole (DBD‐F) as a labelling reagent and α ‐phenylethylamine as an internal...