Determination of psilocybin in hallucinogenic mushrooms by reversed-phase liquid chromatography with fluorescence detection
Talanta January 7, 2005 Kimie Saito, Toshimasa Toyo’oka, Masaru Kato et al. 35 citations
The determination of psilocybin was carried out by reversed-phase liquid chromatography (HPLC) with fluorescence (FL) detection. Psilocybin was labeled with 5-dimethylaminonaphthalene-1-[N-(2-aminoethyl)]sulfonamide (DNS-ED) at 60 degrees C for 4h in the presence of 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide (EDC) as the activation reagent. The resulting derivative was separated on a...