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Synthetic studies of psilocin analogs having either a formyl group or bromine atom at the 5- or 7-position.

Fumio Yamada, Mayumi Tamura, Atsuko Hasegawa, Masanori Somei

Chemical & pharmaceutical bulletin January 2002 DOI: 10.1248/cpb.50.92 (opens in new tab)

Study at a glance

AI-extracted from the abstract
Characteristics Theoretical or philosophical paper Peer reviewed
Topics Psilocybin
Key points The authors report the first preparation of psilocin analogs bearing formyl or bromine groups at the 5- or 7-position, and establish synthetic routes for various brominated indole intermediates and N,N-dimethyltryptamine derivatives.

Abstract

Psilocin analogs having either a formyl group (9-12) or a bromine atom (13-18) at the 5- or 7-position have been prepared for the first time. Syntheses of 5- and 7-bromo derivatives of 4-hydroxy- (23, 24, 28) and 4-benzyloxyindole-3-carbaldehyde (19, 25, 29, 30), 4-benzyloxyindole-3-acetonitriles (20, 31), and 4-benzyloxy-N,N-dimethyltryptamine (32, 34, 35) have also been established.