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Synthesis and evaluation of substituted 2-phenylcyclobutylamines as analogs of hallucinogenic phenethylamines: lack of LSD-like biological activity

David E. Nichols, K. P. Jadhav, Robert Oberlender, Joseph E. Zabik, Josef F. Bossart, Akihiko Hamada, Duane D. Miller

Journal of Medicinal Chemistry September 1, 1984 DOI: 10.1021/jm00375a004 (opens in new tab)

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AI-extracted from the abstract
Characteristics Animal study Peer reviewed
Population Rats
Interventions 4 5-trimethoxyphenyl)cyclobutylamine trans-2-(2 5-dimethoxy-4-methylphenyl)cyclobutylamine 5-dimethoxy-4-methylphenyl)cyclopropylamine
Topics Mescaline LSD
Keywords Phenethylamines Hallucinogen Biological activity Stereochemistry Pharmacology
Citations 12
Key points The cyclobutylamine analogues failed to fully substitute for LSD in a drug discrimination test, indicating they are either less potent or produce different subjective effects.

Abstract

cis- and trans-2-(2,4,5-trimethoxyphenyl)cyclobutylamine and trans-2-(2,5-dimethoxy-4-methylphenyl)cyclobutylamine were synthesized as conformationally restricted analogues of hallucinogenic phenylisopropylamines. In rats trained to discriminate saline from LSD (0.08 mg/kg, ip) in a two-lever drug discrimination paradigm, no generalization of the LSD stimulus to the cis trimethoxy compound occurred at doses up to 20 mg/kg. For both of the trans compounds, partial generalization of the LSD cue occurred at doses of 5 mg/kg or greater. In contrast, complete generalization occurred with trans-2-(2,5-dimethoxy-4-methylphenyl)cyclopropylamine. The ED50 for this compound and the doses of the trans cyclobutyl homologues at which significant drug-appropriate responding occurred indicate that the latter are on the order of 50-75 times less potent than the cyclopropylamine analogue. The lack of generalization to the cyclobutylamines indicates either that their discriminative stimulus properties differ from LSD or that they lack discriminative effects.

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