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Tatsuo Nagasaka

1 paper in the library · 5 citations · publishing 1977

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Synthesis of 4-Substituted Indole Derivatives

Heterocycles 1977 S. Ohki, Tatsuo Nagasaka, Tohru Tuge 5 citations

A general synthetic method of 4-substituted indoles was examined.The Fischer indolization of phenylhydrazones (2, 3, 7, and 8) having chlorine on & position gave 7-chloro-4-substituted indoles (4, 9, and lo), which were converted to 4-substituted indoles (5 and 13) by catalytic hydrogenation.Cyclization of 3-(2-ethoxy~arbonyl-7-chloroindol-4-yl)propionic acid (10) with polyphosphoric acid (PPA)...