Single-crystal structure determination of psilocybin after dehydration.
Acta Crystallographica Section C Structural Chemistry August 7, 2026 Sonya K. Emmett, Lee Cameron, Mark Hestermann et al.
The crystal structure of the known low-temperature anhydrous phase of psilocybin {3-[2-(dimethylamino)ethyl]-1H-indol-4-yl dihydrogen phosphate, C12H17N2O4P} is reported. While the structure was previously characterized using powder X-ray diffraction, this study describes the first determination via single-crystal X-ray diffraction. High-resolution structural models were obtained both before...